표제지
목차
Abstract 8
I. 서론 10
II. 재료 및 방법 15
1. 실험재료 15
2. 실험방법 15
2-1. 표준품 및 시약 15
2-2. 표준용액 조제 16
3. 잔류농약 분석방법 20
3-1. 추출 및 농축 20
3-2. 정제 21
3-3. 기기분석 조건 23
III. 결과 및 고찰 25
1. 분석법 검증 25
1-1. 직선성 25
1-2. 검출한계 및 정량한계 30
1-3. 정확성 30
2. 모니터링 39
IV. 요약 44
V. 참고문헌 46
Table 1. Molecular structures of 16 nonpolar organophosphorus pesticides 17
Table 2. GC-NPD conditions used in the determination of 14... 24
Table 3. Limit of quantitation of 15 nonpolar organophosphorus pesticides 35
Table 4. Recovery results of 14 nonpolar organophosphorus pesticides 36
Table 5. Experimental results of interlaboratory cross-examination... 40
Table 6. Results of the monitoring on inspection of pesticide residues... 43
Figure 1. Experimental flowchart for GC-NPD analysis of 16... 22
Figure 2. Result of GC-NPD analysis for standard chemicals of 15... 27
Figure 3. Blank test of GC-NPD analysis for 15 nonpolar... 28
Figure 4. Result of GC-NPD analysis for 15 nonpolar... 29
Figure 5. Calibration curves of 15 nonpolar organophosphorus... 34