This study was investigated both the Korean oficial soil test method and the international variousmethods for PCBs in soil sample. The analytical guideline of PCBs in contaminated soil were proposed basedon the official soil test methods by discussing the extraction, column cleanup, instrumental conditions, quantificationmethods of peak matching and individual isomers. The total 28 soil samples were selected by consideration ofECD) and gas chromatography/mass spectrometry(GC/MS). In this study, the PCBs were not detected as peakmatching method using GC/ECD, but PCBs detected 0.002~0.487 g/kg using GC/MS in backgroundconcentrations.