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제출문
요약서
Summary
표목차
그림목차
칼라
목차
제1장 서론 18
1.1. 연구의 필요성 및 목적 18
1.2. 이론적 배경 20
1.3. 기본 연구방향 30
1.4. 연구 내용 및 결과 32
제2장 이론적 고찰 35
2.1. STELF process 개요 35
2.2. STELF Process Configuration 38
2.3. Clausius-Clapeyron diagram 분석 48
2.4. IMPEX의 물성 52
제3장 COMPUTER PROGRAMING for DESIGN, MODELING & SIMULATION 54
3.1. Level 0 Design 55
3.2. Level 1 Design 58
제4장 기초실험 67
4.1. 이론적 배경 69
4.2. 실험방법 79
4.3. 실험결과 83
4.4. 결론 및 제언 95
제5장 Bench-scale STELF CHT 97
5.1. STELF Chemical Heat Transformer의 설계 및 제작 97
1. 반응기 설계 및 운전조건 결정 97
2. 부속장치의 설계식 99
5.2. 실험 방법 및 결과 104
1. 실험장치 104
2. 운전방법 120
3. 실험결과 및 고찰 121
가. Pressure-Temperature 선도와 Clausius-Clapeyron 선도[원문불량;p.108] 121
나. 재생실험[원문불량;p.112] 127
다. 출력실험[원문불량;p.121~122,125] 131
라. 모사결과와 실험결과 비교[원문불량;p.127] 143
제6장 STELF Process의 적용 방안 검토 146
6.1. STELF Process의 특성 146
6.2. 적용 업체의 에너지 공정 분석[원문불량;p.135] 151
제7장 결론 159
참고문헌 161
부록 164
[title page etc.]
Contents
Chapter 1. Introduction 18
1.1. Necessities and Objectives of the Research 18
1.2. Theoretical background 20
1.3. Basic direction of the research 30
1.4. Contents and results of the research 32
Chapter 2. Review for theoretical consideration 35
2.1. Summary of STELF process 35
2.2. STELF process configuration 38
2.3. Analysis of Clausius-Clapeyron diagram 48
2.4. The properties of IMPEX 52
Chapter 3. Computer programing for design, modeling and simulation 54
Chapter 4. Basic experiments 67
4.1. Theoretical background 69
4.2. Experimental methods 79
4.3. Experimental results 83
4.4. Conclusions 95
Chapter 5. Bench-scale STELF CHT 97
5.1. Design and Setting of STELF Chemical Heat Transformer 97
1. Reactor design and determination of operating condition 97
2. Design of subsidiary apparatus 99
5.2. Experimental methods and results 104
1. Experimental apparatus 104
2. Operation method 120
3. Experimental results and discussions 121
가. Pressure-Temperature and Clausius-Clapeyron diagram[원문불량;p.108] 121
나. Experiments of Regeneration phase[원문불량;p.112] 127
다. Experiments of production phase[원문불량;p.121~122,125] 131
라. Compare experimental values with calculated values[원문불량;p.127] 143
Chapter 6. Application(Applicaton) of STELF process 146
6.1. Characteristics of STELF process 146
6.2. Analysis of energy flow for manufacturing process of co. which will be applied in STELF system[원문불량;p.135] 151
Chapter 7.conclusion 159
References 161
Appendix 164
(Table 1-1) 냉방·냉동의 영역 구분 및 이용기술 18
(Table 1-2) 냉방·냉동의 기술의 비교 19
(Table 1-3) 물리화학적 축열방법 21
(Table 1-4) 화학반응 사이클의 분류 24
(Table 1-5) STELF process의 계약 체결 현황 29
(Table 2-1) STELF process의 염별 Cp, ΔH, ΔS의 값(이미지참조) 41
(Table 4-1) Surface area of prepared samples 83
(Table 4-2) Various metal loading results 84
(Table 4-3) Apparent density, porosity and average pore diameter of prepared samples 85
(Table 4-4) Total amount of adsorbed NH₃ gas for each samples 86
(Table 5-1) The properties of salt 98
(Table 5-2) Typical properties of Theminol 55 101
(Table 5-4) Specifications of experimental apparatus 111
(Table 6-1) 각 염의 압력별 평형온도 147
(Table 6-2) Generator 염별 필요한 Tm(이미지참조) 148
(Table 6-4) The operation stages of the STELF CTF 157
(Fig. 2-1) The basic unit of STEL system 42
(Fig. 2-2) The operation diagrams of basic unit 43
(Fig. 2-3) A schematic diagram of the basic SLG system 45
(Fig. 2-4) A Clausius-Clapeyron diagram of the CHT with the basic SSG System 48
(Fig. 2-5) Heat Cycle and Reversed Heat Cycle 50
(Fig. 2-6) Relation between apparent density and graphite ratio 53
(Fig. 2-7) Relation between apparent density and volume 53
(Fig. 3-1) The work flow of computer programing 54
(Fig. 3-2) The design procedure of STELF CHT 59
(Fig. 4-1) Flowchart of sample preparation 80
(Fig. 4-2) Schematic diagram of reaction experiment apparatus 82
(Fig. 4-3) TPD profile of expanded graphite according to the temperature ascension : sample No. 1 88
(Fig. 4-4) TPD profile of Ni impregnated expanded graphite according to the temperature ascension : sample No. 2 89
(Fig. 4-5) TPD profile of Ni impregnated expanded graphite according to the temperature ascension : sample No. 3 90
(Fig. 4-6) TPD profile of Ni impregnated expanded graphite according to the temperature ascension : sample No. 4 91
(Fig. 4-7) TPD profile of Mn impregnated expanded graphite according to the temperature ascension : sample No. 5 92
(Fig. 4-8) TPD profile of Ni impregnated expanded graphite according to the temperature ascension : sample No. 6 93
(Fig. 4-9) TPD profile of Ni impregnated expanded graphite according to the temperature ascension : sample No. 7 94
(Fig. 5-1) Experimental apparatus 105
(Fig. 5-2) Picture of experimental apparatus 106
(Fig. 5-3) Detailed drawing(dawing) of engine 107
(Fig. 5-4) Detailed drawing of generator 108
(Fig. 5-5) The positions of thermocouple in experimental apparatus 110
(Fig. 5-6) The actual and instrumental measure according to pump speed in engine 114
(Fig. 5-7) The actual and instrumental measure according to pump speed in generator 115
(Fig. 5-8) The preliminary test of MFC 117
(Fig. 5-9) The heat capacity according to temperature in thermonol 55 118
(Fig. 5-10) The density according to temperature in thermonol 55 119
(Fig. 5-11) The P-T diagram for engine salt 122
(Fig. 5-12) The Clausius-Clapeyron diagram for engine salt 124
(Fig. 5-13) The P-T diagram for generator salt[원문불량;p.108] 125
(Fig. 5-14) The Clausius-Clapeyron diagram for generator salt 126
(Fig. 5-15) The temperature difference of block according to elapsed time 128
(Fig. 5-16) The pressure difference of reactor according to elapsed time[원문불량;p.112] 129
(Fig. 5-17) The temperature difference of working fluid according to elapsed time 130
(Fig. 5-18) The mean power as a function of the number of times of experiment at production process 132
(Fig. 5-19) The total energy as a function of regeneration time 134
(Fig. 5-20) The output power according(acoording) to elapsed time in variation of regeneration time 135
(Fig. 5-21) The power according(acoording) to elapsed time 137
(Fig. 5-22) The block temperature according(acoording) to elapsed time[원문불량;p.121] 138
(Fig. 5-23) The reactor pressure according(acoording) to elapsed time[원문불량;p.122] 139
(Fig. 5-24) The block temperature as a function of initial pressure 141
(Fig. 5-25) The reactor pressure as a function of initial pressure[원문불량;p.125] 142
(Fig. 5-26) Evaluated reaction rate for generator synthesis[원문불량;p.127] 144
(Fig. 5-27) Comparison(Comparision) of the block temperature between calculated and experimental value 145
(Fig. 6-1) 양영제지의 에너지 흐름도[원문불량;p.135] 152
(Fig. 6-2) 양영제지의 보일러 보충수의 flow diagram 153
(Fig. 6-3) The process diagram of Dong Sin Special Steel Co. 155
(Fig. 6-4) Clausius-Clapeyron diagram of STELF CTF 156
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