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Part I

Synthesis of Bulk Materials 1

Chapter 1

Flame Hydrolysis for Oxide Supports 3

Dieter Kerner

Chapter 2

Amine-Assisted Synthesis of Aluminum Oxide 15

Alexander I. Kozlov, Mayfair C. Kung, Wen-Mei Xue,

Harold H. Kung, and Shandong Yuan

Chapter 3

Aerogel Synthesis 31

Gerard M. Pajonk '

Chapter 4

Fine-Tuning the Functionalization of Mesoporous Silica 45

Hung-Ting Chen, Seong Huh, and Victor S.-Y. Lin

Chapter 5

The Environmentally Friendly Synthesis of Heteropolyacids 75

Graciela M. Valle, Silvana R. Matkovic,

Luis A. Gambaro, and Laura E. Briand

Chapter 6

Synthesis of Metal Colloids 93

Lawrence D'Souza and Ryan Richards

Part II

Synthesis of Heterogeneous Catalysts 139

Chapter 7

Microwave-Assisted Synthesis of Nanolayer Carbides and Nitrides 141

Justin Bender, Jennifer Dunn, and Ken Brezinsky

Chapter 8

Sol-Gel Synthesis of Supported Metals 163

Benozt Heinrichs, Stephanie Lambert, Nathalie Job, and Jean-Paul Pirard

Chapter 9

Synthesis of Supported Metal Catalysts by Dendrimer-Metal Precursors 209

D. Samuel Deutsch, Christopher T. Williams, and Michael D. Amiridis

Chapter 10

Synthesis of Oxide- and Zeolite-Supported Catalysts from

Organometallic Precursors 237

Bruce C. Gates

Chapter 11

Supported Metal Oxides and the Surface Density Metric 251

William -v. Knowles, Michael O. Nutt, and Michael S. Wong

Chapter 12

Solid-State Ion-Exchange of Zeolites 283

Geoffrey L. Price

Chapter 13

Strong Electrostatic Adsorption of Metals onto Catalyst Supports 297

John R. Regalbuto

Chapter 14

Deposition-Precipitation Synthesis of Supported Metal Catalysts 319

Catherine Louis

Chapter 15

Production of Supported Catalysts by Impregnation and (Viscous) Drying 341

John w: Geus

Part III

Catalyst Finishing 373

Chapter 16

Drying of Supported Catalysts 375

Azzeddine Lekhal, Benjamin J. Glasser, and Johannes G. Khinast

Chapter 17

The Effects of Finishing and Operating Conditions on Pt

Supported Catalysts during CO Oxidation 405

Eduardo E. Wolf

Chapter 18

Catalysts for New Uses: Needed Preparation Advances 449

Bernard Delmon Index 465

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Catalyst preparation : science and engineering 이용현황 표 - 등록번호, 청구기호, 권별정보, 자료실, 이용여부로 구성 되어있습니다.
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Improving the effectiveness of catalysts is the best way to ensure cleaner, more efficient industrial processes for a wide range of applications. Catalyst Preparation: Science and Engineering explores the optimization of catalytic materials through traditional and novel methods of catalyst preparation, characterization, and monitoring on laboratory and industrial scales.

The book presents many key principles of heterogeneous catalyst preparation and the methods used to synthesize a catalyst with a particular composition and morphology. The first chapters examine the synthesis of bulk materials including amorphous and mesoporous oxide supports, heteropolyacids, and colloidal metals. Subsequent chapters focus on the syntheses of heterogeneous nanoscale materials, including those based on metal complex?substrate interactions and those using non-interacting precursors via viscous drying. The final chapters concentrate on pretreatment, drying, and finishing effects before concluding with a prognosis on future applications involving catalyst preparation and the technological advances necessary for continued progress.

An ideal companion for scientists exploring the preparation of application-specific catalysts based on desired catalytic properties, Catalyst Preparation: Science and Engineering provides a balanced overview of important synthesis parameters to consider for good catalyst design.

This text explores the optimization of catalytic materials through traditional and novel methods of catalyst preparation, characterization, and monitoring for oxides, supported metals, zeolites, and heteropolyacids. It focuses on the synthesis of bulk materials and of heterogeneous materials, particularly at the nanoscale. The final chapters examine pretreatment, drying, finishing effects, and future applications involving catalyst preparation and the technological advances necessary for continued progress. Topics also include heat and mass transfer limitations, computation methods for predicting properties, and catalyst monitoring on laboratory and industrial scales.

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