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Acknowledgements
1 Introduction 1
1.1 The discovery of fullerene-related carbon nanotubes 3
1.2 Characteristics of multiwalled nanotubes 4
1.3 Single-walled nanotubes 7
1.4 Pre-1991 evidence for carbon nanotubes 10
1.5 Nanotube research 12
1.6 Organisation of the book 13
2 Synthesis: Preparation methods, growth mechanisms and processing techniques 16
2.1 Production of multiwalled nanotubes: non-catalytic methods 18
2.2 Experiments on the heat treatment of fullerene soot 25
2.3 Catalytically produced multiwalled nanotubes 28
2.4 Nanotubes on TEM support grids: a word of warning 34
2.5 Single-walled nanotubes 37
2.6 Theories of nanotube growth 43
2.7 Purification of multiwalled tubes 49
2.8 Purification of single-walled tubes 52
2.9 Alignment of nanotube samples 53
2.10 Length control of carbon nanotubes 53
3 Structure 61
3.1 Classification of tubular biological structures 62
3.2 Bonding in carbon materials 65
3.3 The structure of carbon nanotubes: theoretical discussion 66
3.4 The physical stability of carbon nanotubes 82
3.5 Experimental studies of nanotube structure: multiwalled nanotubes 82
3.6 Experimental studies of nanotube structure: single-walled nanotubes 98
3.7 Structure of carbon nanoparticles 102
3.8 Nanocones 104
4 The physics of nanotubes 111
4.1 Electronic properties of graphite and carbon fibres 112
4.2 Electronic properties of nanotubes: theory 115
4.3 Electronic properties of nanotubes: experimental measurements 123
4.4 Magnetic properties of nanotubes 137
4.5 Optical properties of nanotubes 140
4.6 Vibrational properties of nanotubes 141
4.7 Electron energy loss spectroscopy of nanotubes 147
4.8 Nanotube field emitters 149
5 Nanocapsules and nanotest-tubes 156
5.1 Metallofullerenes 157
5.2 Filling nanotubes and nanoparticles by arc-evaporation 158
5.3 Preparation of filled nanoparticles from microporous carbon 162
5.4 Properties of filled nanoparticles 164
5.5 Technegas 166
5.6 Opening and filling of nanotubes using chemical methods and capillarity 166
5.7 Filling of single-walled nanotubes 178
5.8 Storing gases in nanotubes 180
6 The ultimate carbon fibre? The mechanical properties of carbon nanotubes 186
6.1 Conventional carbon fibres 187
6.2 Graphite whiskers 188
6.3 Catalytically grown carbon fibres 190
6.4 Mechanical properties of carbon nanotubes 191
6.5 Carbon nanotube composites 200
6.6 Nanotubes as tips for scanning probe microscopes 207
7 Curved crystals, inorganic fullerenes and nanorods 213
7.1 Chrysotile and imogolite 214
7.2 Inorganic fullerenes from layered metal dichalcogenides 218
7.3 Nanotubes and nanoparticles containing boron and nitrogen 223
7.4 Carbide nanorods 229
8 Carbon onions and spheroidal carbon 235
8.1 Carbon onions 235
8.2 Spheroidal carbon particles in soot 246
8.3 Spherulitic graphite cast iron 254
8.4 Spheroidal structures in mesophase pitch 260
9 Future directions 266
9.1 Towards a carbon nanotube chemistry 267
9.2 New all-carbon structures 269
9.3 Nanotubes in nanotechnology 270
9.4 Final thoughts 270
Name index 275
Subject index 277
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