표제지
목차
I. 서론 7
II. 재료 및 방법 10
실험 재료 10
실험 방법 10
실험기기 및 분석조건 12
통계분석방법 15
III. 결과 16
유기인계및 피레스로이드계 Chromatogram 16
생체시료 분석결과 17
IV. 결론 21
V. 참고문헌 22
VI. Abstracts 25
Table 1. Retention time and fragment ions of the dialkyl phosphates 13
Table 2. Retention time and fragment ions derivatives of metabolites of pyrethroid metabolites 13
Table 3. The operating conditions of GC/MSD for organophosphate pesticides 14
Table 4. The operating conditions of GC/MSD for pyrethroids pesticides 15
Table 5. The concentration of metabolites for organophosphates and pyrethroids according to flowers worker(ug/g creatinine)[median(min-max)] 18
Table 6. The result of correlation analysis of concentration metabolites of organophosphate 19
Table 7. The result of correlation analysis of concentration metabolites of pyrethroids 19
Table 8. The detection rates of metabolites of organophosphate and pyrethroids 20
Fig 1. Retention time of after spiking dialkylphosphates-PFBBr at urine. 16
Fig 2. Retention time of after spiking pyrethroid-MTBSTFA at urine. 17