Section 1 분석일반 / 1제1장 분석을 위한 기초 / 31-1 분석데이터 평가 ············································································································· 31-1-1 오차 ························································································· 31-1-2 정확도와 정밀도 ··································································· 51-1-3 Q Test ················································································ 111-1-4 최소제곱법 (Least Square Method) ······························ 121-1-5 감도와 검출한계 ································································ 161-1-6 유효숫자 ·············································································· 201-2 단위환산 및 명명법 ····································································································· 241-2-1 단위계 ················································································· 241-2-2 단위환산 ·············································································· 261-2-3 무기화합물의 명명법 ························································· 271-3 화학분석 ························································································································ 281-3-1 개요 ······················································································· 281-3-2 화학분석의 분류 ································································ 291-3-3 화학분석의 일반적 단계 ··················································· 321-3-4 부피분석 ·············································································· 44제2장 대한민국약전 실험의 기초 / 572-1 기초준비 ························································································································ 572-1-1 기구와 시약 ········································································ 572-1-2 무게(질량)의 측정 ····························································· 652-1-3 부피의 측정 ·········································································· 692-2 기초의약분석실험 ········································································································· 792-2-1 서론 ······················································································· 792-2-2 실험에서의 일반적인 주의사항 ·········································· 802-2-3 실험노트 기록방법 ····························································· 842-2-4 실험보고서 종류 ································································ 852-2-5 실험보고서 작성 요령 ························································· 852-3 대한민국약전 ·············································································································· 1012-3-1 약전의 의미 ········································································ 1012-3-2 의약품의 규격 ···································································· 1022-3-3 약전의 역사 ···································································· 1052-3-4 대한민국약전 통칙 ···························································· 1072-3-5 대한민국약전 일반시험법 (일부발췌) ··························· 135Section2 의약품 기기분석/177제1장 전자기 복사선과 광학 / 1791-1 개론 ····························································································································· 1791-2 전자기 복사선의 파동성 ··························································································· 1811-3 전자기 복사선의 입자성 ··························································································· 1831-4 Beer의 법칙 ··············································································································· 188제2장 자외-가시부 흡광광도법 / 1912-1 개론 ····························································································································· 1912-2 정성분석 ····················································································································· 1922-2-1 용매 ················································································· 1942-2-2 흡수스펙트럼 작성 ························································· 1952-3 정량분석 ····················································································································· 1962-3-1 Beer 법칙 ········································································· 1972-3-2 Beer 법칙의 문제점 ························································ 2002-3-3 정확도와 정밀도 ······························································ 2022-3-4 정량 과정에서 야기되는 오차 ········································ 2052-3-5 분광 측정 오차 ································································ 2072-3-6 일반적 정량과정 ······························································ 2092-3-7 혼합물의 정량 ·································································· 212-4 측정 장치 및 기기 ····································································································· 2142-4-1 광원 ··················································································· 2162-4-2 파장선택부 ········································································ 2172-4-3 시료부 (흡수용기, cell) ·············································· 2212-4-4 검출기 (detector) ··························································· 2222-4-5 광학계 ················································································· 2232-5 정량분석에의 응용 ····································································································· 2242-5-1 정량법의 종류 ····················································································· 2242-6 대한약전 의약품각조에의 응용 ················································································ 2322-6-1 확인시험 ············································································· 2322-6-2 시성치로서의 ································································ 2342-6-3 순도시험 ·········································································· 2342-6-4 정량법 ··············································································· 235제3장 크로마토그래피 / 2413-1개론 ······························································································································· 2413-2 크로마토그래피법의 기초이론 ·················································································· 2453-2-1 이론단수(N) 및 유효이론단수(Neff) ····························· 2463-2-2 이론단 칼럼높이 (Height Equivalent to a Theoretical Plate) 2473-2-3 칼럼의 용량인자(capacity factor 혹은 retention factor: k') 2523-2-4 분리계수/분리인자 (separation factor : α) ··················· 2533-2-5 분리도 (Resolution Function: RS) ······························· 2533-2-6 분리능의 최적비 ······························································ 2563-3 가스크로마토그래피 (GC) ························································································ 2563-3-1 장치 ······································································································ 2563-4 고성능액체크로마토그래피(HPLC) ·········································································· 2703-4-1 HPLC의 특징 ····································································· 2713-4-2 장치의 개요 ········································································ 2713-4-3 크로마토그래피 분리 메커니즘 ········································ 3173-4-5 이동상 용매의 선택 ··························································· 3573-4-6 이동상의 제조 ·································································· 3653-4-7 시료의 분석 ········································································ 373Section 3 기타 물리분석 및 측광분석 / 397제1장 pH 측정법 / 3991-1 전기화학(Electrochemistry)개론 ··········································································· 3991-1-1 산화/환원반응 (Redox Reaction) ·································· 4001-1-2 산화환원전위 (Oxidation Reduction potential ; ORP) 4011-1-3 전기화학 셀과 표준수소전극(standard hydrogen electrode) 4051-1-4 표준전극전위 (Standard electrode potential) ············ 4081-1-5 전극전위 표현법 ······························································ 4121-2 Nernst 식 ··················································································································· 4131-3 pH와 수소이온농도 [H+] ······················································································ 4171-3-1 물의 해리(전리)와 pH ······················································ 4181-3-2 pH electrode (pH 전극) ·················································· 4211-3-3 pH meter의 보정(Calibration) 및 측정 응용 ·············· 4241-3-4 간단한 용액의 pH 계산 ·················································· 430제2장 선광도 (Optical Rotation) 측정 / 4352-1 빛의 평면편광 ········································································································ 4362-1-1 편광자(polarizer)와 검광자(Analyzer) ························· 4372-1-2 선광도(Optical rotation)와 선광계(Polarimeter) ······· 4382-2 이성질체(Isomer) ·································································································· 4392-2-1 구조이성질체 (2차원, 평면적) ···································· 4402-2-2 입체이성질체 (3차원, 입체적) ······································ 4422-3 선광도 및 비선광도의 측정 ······················································································ 4482-3-1 편광계 장치의 구성과 측정원리 ···································· 4482-3-2 선광도의 측정 ·································································· 4502-3-3 ORD, CD 분광광도계 ···················································· 454제3장 적외부 분광광도법 / 4573-1 분자의 적외선 흡수 ··································································································· 4593-2 분자의 진동 ················································································································ 4613-3 분자진동의 파수 (ν) ································································································· 4643-4 적외선 흡수스펙트럼의 분석에의 응용 ··································································· 4683-4-1 정성분석 및 화합물 구조 추정 ······································ 4683-4-2 적외선 스펙트럼 해석의 기초 ········································ 4723-4-3 정량분석 ·········································································· 4753-5 적외선 분광광도계 장치 ··························································································· 4773-5-1 분산형 적외선 분광광도계 ··········································· 4783-5-2 간섭형 적외선 분광광도계(FTIR) ······························· 4833-5-3 비분산 적외선분석기(NDIR) ········································ 4853-5-4 시료의 취급 및 측정 ····················································· 48