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The computer-aided design/computer-aided manufacturing (CAD/CAM) system was introduced to shorten the production time of all-ceramic restorations and the number of patient visits. Among these types of ceramic for dental CAD/CAM, they have been processed into inlay, onlay, and crown shapes using leucite-reinforced glass-ceramics to improve strength. The purpose of this study was to observe the mechanical properties and microstructure of leucite-reinforced glass-ceramics for dental CAD/CAM. Two types of leucite-reinforced glass-ceramic blocks (IPS Empress CAD, Rosetta BM) were prepared with diameter of 13 mm and thickness of 1 mm. Biaxial flexural testing was conducted using a piston-on-three-ball method at a crosshead speed of 0.5 mm/min. Weibull statistics were used for the analysis of biaxial flexural strength. Fracture toughness was obtained using an indentation fracture method. Specimens were observed by field emission scanning electron microscopy to examine the microstructure of the leucite crystalline phase after acid etching with 0.5% hydrofluoric acid aqueous solution for 1 minute. The results of strength testing showed that IPS Empress CAD had a mean value of 158.1±8.6 MPa and Rosetta BM of 172.3±8.3 MPa. The fracture toughness results showed that IPS Empress CAD had a mean value of 1.28±0.19 MPa·m¹/² and Rosetta BM of 1.38±0.12 MPa·m¹/². The Rosetta BM sample exhibited higher strength and fracture toughness. Moreover, the crystalline phase size and ratio were increased in the Rosetta BM sample. The above results are expected to elucidate the basic mechanical properties and crystal structure characteristics of IPS Empress CAD and Rosetta BM. Additionally, they will help develop leucite-reinforced glass-ceramic materials for CAD/CAM.
번호 | 참고문헌 | 국회도서관 소장유무 |
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1 | Relationship between elastic and mechanical properties of dental ceramics and their index of brittleness ![]() |
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2 | Properties and Clinical Application of Three Types of Dental Glass-Ceramics and Ceramics for CAD-CAM Technologies ![]() |
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3 | Influence of Low Temperature Degradation on Bond Strength of Yttria-Stabilized Tetragonal Zirconia Polycrystal Core to Veneering Ceramic | 소장 |
4 | Advances in dental ceramics. ![]() |
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5 | Evolution of dental ceramics in the twentieth century ![]() |
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6 | Sakaguchi RL, Powers JM: Craig's restorative dental materials. 13th ed. Elsevier Mosby, Philadelphia, pp.455-462, 2012. | 미소장 |
7 | Holand W, Beall GH: Glass-ceramic technology. 2nd ed. Wiley, Hoboken, 2012. | 미소장 |
8 | Clinical performance of bonded leucite-reinforced glass ceramic inlays and onlays after eight years. ![]() |
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9 | Miyazaki T, Hotta Y, Kunii J, Kuriyama S, Tamaki Y: A review of dental CAD/CAM: current status and future perspectives from 20 years of experience. Dent Mater J 28: 44-56, 2009. https://doi.org/10.4012/dmj.28.44 | 미소장 |
10 | Trost L, Stines S, Burt L: Making informed decisions about incorporating a CAD/CAM system into dental practice. J Am Dent Assoc 137 Suppl: 32S-36S, 2006. https://doi.org/10.14219/jada.archive.2006.0399 | 미소장 |
11 | Crystallization and flexural strength optimization of fine-grained leucite glass-ceramics for dentistry ![]() |
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12 | Quinn GD, Giuseppetti AA, Hoffman KH: Chipping fracture resistance of dental CAD/CAM restorative materials: part I--procedures and results. Dent Mater 30: e99-e111, 2014. https://doi.org/10.1016/j.dental.2014.02.010 | 미소장 |
13 | Translucency and biaxial flexural strength of four ceramic core materials ![]() |
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14 | Anstis GR, Chantikul P, Lawn BR, Marshall DB: A critical evaluation of indentation techniques for measuring fracture toughness: I, Direct crack measurements. J Am Ceram Soc 64: 533-538, 1981. https://doi.org/10.1111/j.1151-2916.1981.tb10320.x | 미소장 |
15 | Im YW, Jun SK, Kim SC, et al.: Standardized test methods for mechanical properties of dental prosthetic/restorative materials and their applications. Korean J Dent Mater 42: 259-270, 2015. https://doi.org/10.14815/kjdm.2015.42.3.259 | 미소장 |
16 | Fracture toughness of two lithium disilicate dental glass ceramics ![]() |
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17 | Sin CH, Hwang SS, Han GS: Shear bond strength of veneering ceramic and zirconia core according to the surface treatments. J Dent Hyg Sci 13: 487-492, 2013. | 미소장 |
18 | Kim KB, Kim JH: A study on the shear bond strength of veneering ceramics to the lithium disilicate (IPS e.max CAD) core. J Dent Hyg Sci 13: 290-295, 2013. | 미소장 |
19 | The fracture resistance of a CAD/CAM Resin Nano Ceramic (RNC) and a CAD ceramic at different thicknesses ![]() |
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20 | Surface morphology and fracture in handpiece adjusting of a leucite-reinforced glass ceramic with coarse diamond burs ![]() |
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21 | Dynamic fatigue and strength characterization of three ceramic materials ![]() |
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22 | Flexure Tests on Dental Ceramics ![]() |
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23 | Influence of Test Method on Failure Stress of Brittle Dental Materials ![]() |
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24 | A systematic review of the cost of data collection for performance monitoring in hospitals ![]() |
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25 | Lin WS, Ercoli C, Feng C, Morton D: The effect of core material, veneering porcelain, and fabrication technique on the biaxial flexural strength and weibull analysis of selected dental ceramics. J Prosthodont 21: 353-362, 2012. https://doi.org/10.1111/j.1532-849X.2012.00845.x | 미소장 |
26 | Weibull analysis and flexural strength of hot-pressed core and veneered ceramic structures ![]() |
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27 | A statistical approach to the mechanical testing of dental materials ![]() |
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28 | Fracture behavior of lithia disilicate- and leucite-based ceramics ![]() |
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29 | Harrer W, Danzer R, Morrell R: Influence of surface defects on the biaxial strength of a silicon nitride ceramic: increase of strength by crack healing. J Eur Ceram Soc 32: 27-35, 2012. https://doi.org/10.1016/j.jeurceramsoc.2011.07.019 | 미소장 |
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