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K₂SnCl₆ single crystals doped with Cu were grown by the evaporation of saturated solution. The electron magnetic resonance (EMR) of the Cu²+ ion in the crystal has been investigated by using an X-band spectrometer. The rotation pattern in the crystallographic plane together with spin Hamiltonian parameters of Cu²+ ion in K₂SnCl₆:Cu single crystal shows that the local site symmetry of the Cu²+ ion is cubic at room temperature. The calculated spectroscopic splitting factor g of Cu²+ impurity ion is 2.1908(±0.0007). The hyperfine constants of Cu²+ impurity ion due to the 63Cu and 65Cu isotopes in K₂SnCl₆:Cu crystal are 0.83(±0.01)×10−4 cm−1 and 0.89(±0.01)×10−4 cm−1, respectively. It turns out that the Cu²+ ion substitutes for the K+ ion without any nearby charge compensation.

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기사명 저자명 페이지 원문 목차
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참고문헌 (19건) : 자료제공( 네이버학술정보 )

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번호 참고문헌 국회도서관 소장유무
1 R. G. Dickinson, J. Am. Chem. Soc. 44, 276 (1922). 미소장
2 J. H. M. Thornley, J. Phys. C 1, 1024 (1968). 미소장
3 A. J. Lindop, J. Phys. C.: Sol. State Phys. 3, 1984 (1970). 미소장
4 A. Abragam and B. Bleaney, Electron paramagnetic resonance of transition ions (Clarendon Pres, Oxford) 1970. 미소장
5 T. L. Brown, Jr. W. G. McDugle, and L. G. Kent, J. Am. Chem. Soc. 92, 12 (1970). 미소장
6 D. Nakamura, R. Ikeda, and M. Kubo, Co-ordination Chemistry Revices 17, 281 (1975). 미소장
7 R. L. Armstrong, J. D. Mintz, and M. D'Iorio, Phys. Rev. Lett. 44, 747 (1980). 미소장
8 C. Dimitropoulos, J. J. Van der Klink, J. Pelzl, M. Regelsberger, and K. Rossler, Proc. Faraday Symposium 13 Pulsed NMR in Solids (1978, ed. D. A. Young). 미소장
9 J. J. Van der Klink and C. Dimitropoulus, J. Mol. Str. 58, 359 (1980). 미소장
10 J. Pelzl, V. Waschk, Y. M. Seo, and C. Dimitropoulos, J. Mol. Str. 111, 363 (1983). 미소장
11 A. Sasane, D. Nakamura, and M. Kubo, J. Mag. Res. 3, 76 (1970). 미소장
12 K. R. Jeffrey, J. Mag. Res. 7, 184 (1972). 미소장
13 R. G. Dickinson, J. Am. Chem. Soc. 44, 276 (1922). 미소장
14 H. Boysen, J. Ihringer, W. Prandl, and W. Yelon, Solid State Commun. 20, 1019 (1976). 미소장
15 A. Sasane, D. Nakamura, and M. Kubo, J. Mag. Res. 3, 76 (1970). 미소장
16 K. R. Jeffrey, J. Mag. Res. 7, 184 (1972). 미소장
17 S. Altschuler and B. M. Kozyrev, Electron Paramagnetic Resonance in Compounds of Transition Elements (Wiley, New York, 1974) Chap. 3. 미소장
18 S. K. Misra and C. Rudowicz, Phys. Stat. Sol. (b) 147, 677 (1988). 미소장
19 CRC Handbook of Chemistry and Physics, 76th ed., edited by D. R. Lide (CRC Press, Boca Raton, NY, London, Tokyo, 1995-1996), p 11-49. 미소장

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